Strategic Optimization of the Middle Domain IIIA in RBP-Albumin IIIA-IB Fusion Protein to Enhance Productivity and Thermostability

Int J Mol Sci. 2024 Dec 27;26(1):137. doi: 10.3390/ijms26010137.

Abstract

The protein therapeutics market, including antibody and fusion proteins, has experienced steady growth over the past decade, underscoring the importance of optimizing amino acid sequences. In our previous study, we developed a fusion protein, R31, which combines retinol-binding protein (RBP) with albumin domains IIIA and IB, linked by a sequence (AAAA), and includes an additional disulfide bond (N227C-V254C) in IIIA. This fusion protein effectively inhibited hepatic stellate cell activation. In this study, we further optimized the sequence. The G176K mutation at the C-terminus of RBP altered the initiation site of the first α-helix in domain IIIA, shifting it from P182 to K176, and promoted polar interactions between K176 and adjacent residues, enhancing the rigidity of the RBP/IIIA interface. The introduction of an additional disulfide bond (V231C/Y250C) connecting helices 3 and 4 in IIIA resulted in a three-fold increase in productivity and a 2 °C improvement in thermal stability compared to R31. Furthermore, combining the G176K mutation with V231C/Y250C further enhanced both productivity and anti-fibrotic activity. These findings suggest that the enhanced stability of domain IIIA, conferred by V231C/Y250C, along with the increased rigidity of the RBP/IIIA interface, optimizes interdomain distance and alignment, facilitating proper protein folding.

Keywords: fibrosis; fusion protein; productivity; structural rigidity; thermal stability.

MeSH terms

  • Albumins / chemistry
  • Albumins / metabolism
  • Amino Acid Sequence
  • Animals
  • Hepatic Stellate Cells / metabolism
  • Humans
  • Mice
  • Models, Molecular
  • Mutation
  • Protein Domains
  • Protein Stability*
  • Rats
  • Recombinant Fusion Proteins* / chemistry
  • Recombinant Fusion Proteins* / genetics
  • Recombinant Fusion Proteins* / metabolism
  • Retinol-Binding Proteins / chemistry
  • Retinol-Binding Proteins / genetics
  • Retinol-Binding Proteins / metabolism

Substances

  • Recombinant Fusion Proteins
  • Retinol-Binding Proteins
  • Albumins

Grants and funding