Mechanism of sensor kinase CitA transmembrane signaling

Nat Commun. 2025 Jan 22;16(1):935. doi: 10.1038/s41467-024-55671-3.

Abstract

Membrane bound histidine kinases (HKs) are ubiquitous sensors of extracellular stimuli in bacteria. However, a uniform structural model is still missing for their transmembrane signaling mechanism. Here, we used solid-state NMR in conjunction with crystallography, solution NMR and distance measurements to investigate the transmembrane signaling mechanism of a paradigmatic citrate sensing membrane embedded HK, CitA. Citrate binding in the sensory extracytoplasmic PAS domain (PASp) causes the linker to transmembrane helix 2 (TM2) to adopt a helical conformation. This triggers a piston-like pulling of TM2 and a quaternary structure rearrangement in the cytosolic PAS domain (PASc). Crystal structures of PASc reveal both anti-parallel and parallel dimer conformations. An anti-parallel to parallel transition upon citrate binding agrees with interdimer distances measured in the lipid embedded protein using a site-specific 19F label in PASc. These data show how Angstrom scale structural changes in the sensor domain are transmitted across the membrane to be converted and amplified into a nm scale shift in the linker to the phosphorylation subdomain of the kinase.

MeSH terms

  • Bacterial Proteins / chemistry
  • Bacterial Proteins / metabolism
  • Cell Membrane / metabolism
  • Citric Acid / chemistry
  • Citric Acid / metabolism
  • Crystallography, X-Ray
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Histidine Kinase / chemistry
  • Histidine Kinase / genetics
  • Histidine Kinase / metabolism
  • Membrane Proteins / chemistry
  • Membrane Proteins / metabolism
  • Models, Molecular
  • Phosphorylation
  • Protein Domains
  • Protein Kinases / chemistry
  • Protein Kinases / metabolism
  • Signal Transduction*

Substances

  • Citric Acid
  • Histidine Kinase
  • Bacterial Proteins
  • Protein Kinases
  • Membrane Proteins