Isolation and general characterization of a heat-stable proteinase from Pseudomonas fluorescens aft 36

Biochim Biophys Acta. 1982 Aug 6;717(2):376-83. doi: 10.1016/0304-4165(82)90192-1.

Abstract

An extracellular proteinase from Pseudomonas fluorescens, strain AFT 36, was isolated to homogeneity by chromatography on DEAE-cellulose and Sephadex G-150; a 230-fold increase in specific activity with a recovery of 53% was obtained. The enzyme was optimally active at pH 6.5 and 45 degrees C; activity declined rapidly at higher temperatures but significant activity persisted down to 4 degrees C. Activity was strongly inhibited by 10(-3) M EDTA and was partially restored by addition of Zn2+, Ca2+ or Co2+. The Km values on methylated casein and sodium caseinate were 18.2 and 7.1 mg/ml, respectively. The enzyme was very labile in phosphate buffer and in a mild salts buffer at 55 degrees C but was very stable in the latter at more than 80 degrees C.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cations, Divalent
  • Edetic Acid / pharmacology
  • Kinetics
  • Metals / pharmacology
  • Peptide Hydrolases / isolation & purification*
  • Peptide Hydrolases / metabolism
  • Pseudomonas / enzymology
  • Pseudomonas fluorescens / enzymology*
  • Species Specificity

Substances

  • Cations, Divalent
  • Metals
  • Edetic Acid
  • Peptide Hydrolases