Mutations at the C-terminal isoleucine and other potential iron ligands of 5-lipoxygenase

Eur J Biochem. 1995 Jun 1;230(2):401-7. doi: 10.1111/j.1432-1033.1995.0401h.x.

Abstract

The non-heme iron centre in human 5-lipoxygenase was studied. Recombinant enzyme was expressed in Escherichia coli, purified and assayed for iron content and enzyme activity. For non-mutated enzyme, the iron content was 1.01 +/- 0.19 mol/mol. Deletion of the C-terminal Ile673 resulted in an iron content of 0.03 +/- 0.07 mol/mol and undetectable lipoxygenase activity. Mutations at His367, Glu376 and Asn554 led to drastically decreased enzyme activity (< 2% of non-mutated control) but iron was still present. In addition to Glu376, eight other conserved acidic residues (Asp/Glu) in 5-lipoxygenase were replaced, none of which was crucial for enzyme activity. We conclude that Ile673 is an iron ligand in 5-lipoxygenase, while our results do not support that Glu376 or Asn554 have this function. The possible role of His367 as a replaceable iron ligand is discussed.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Arachidonate 5-Lipoxygenase / genetics*
  • Arachidonate 5-Lipoxygenase / metabolism
  • Cloning, Molecular
  • Escherichia coli / genetics
  • Humans
  • Iron / metabolism*
  • Isoleucine / genetics*
  • Isoleucine / metabolism
  • Ligands
  • Mutagenesis, Site-Directed

Substances

  • Ligands
  • Isoleucine
  • Iron
  • Arachidonate 5-Lipoxygenase