Distribution of surface-exposed and non-accessible amino acid sequences among the two major structural domains of the S-layer protein of Aeromonas salmonicida

J Mol Biol. 1993 Oct 20;233(4):753-65. doi: 10.1006/jmbi.1993.1550.

Abstract

The tetragonally arranged crystalline surface protein array (A-layer) of the fish pathogenic bacterium Aeromonas salmonicida is a virulence factor. Circular dichroism studies in the presence or absence of 0.1% sodium dodecyl sulfate showed that the secondary structure of A-protein, and its 39,439 molecular weight amino-terminal trypsin-resistant peptide, were altered. In both cases alpha-helix was increased significantly at the expense of beta-structure when SDS was added. Western and dot immunoblotting, immuno-microscopy and enzyme-linked immunosorbent assay with monospecific polyclonal antiserum and eight monoclonal antibodies specific for epitopes exposed on the surface of native A-layer showed that the 481 residue A-protein subunit and the surface of A-layer were conserved antigenically. Mimeotope analysis of nonapeptides representing the sequence of A-protein allowed identification of 146 residues in presumed linear epitopes accessible on the surface of A-layer. Inaccessible or non-epitopic residues accounted for 70% of the protein. The majority of inaccessible residues were in the N-terminal 301 residues of A-protein. Dispersed among these were 65 surface-accessible residues in five linear epitope clusters illustrating the complex folding of this major structural domain of A-protein. The C-terminal 180 residues carried fewer linear epitopes but contained the major region of A-layers surface-accessible sequence, including four linear epitopes in predominantly hydrophobic sequence. Four A-layer surface-binding monoclonal antibodies also bound to this minor structural domain, although the epitopes of only two were identified by mimeotope analysis. The epitopes of six A-layer surface-binding monoclonals could not be identified, suggesting that A-layer may also contain conformation dependent surface epitopes.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Aeromonas / chemistry*
  • Amino Acid Sequence
  • Animals
  • Antigens, Bacterial / chemistry*
  • Bacterial Outer Membrane Proteins / chemistry*
  • Bacterial Proteins*
  • Blotting, Western
  • Circular Dichroism
  • Enzyme-Linked Immunosorbent Assay
  • Epitopes / chemistry
  • Fluorescent Antibody Technique
  • Humans
  • Membrane Glycoproteins*
  • Microscopy, Electron
  • Molecular Sequence Data
  • Molecular Weight
  • Protein Structure, Secondary
  • Trypsin
  • Ultracentrifugation

Substances

  • Antigens, Bacterial
  • Bacterial Outer Membrane Proteins
  • Bacterial Proteins
  • Epitopes
  • Membrane Glycoproteins
  • S-layer proteins
  • Trypsin