Expression of human interferon omega 1 in Sf9 cells. No evidence for complex-type N-linked glycosylation or sialylation

Eur J Biochem. 1993 Nov 1;217(3):913-9. doi: 10.1111/j.1432-1033.1993.tb18321.x.

Abstract

Human interferon omega 1 (IFN-omega 1) was expressed in Spodoptera frugiperda Sf9 insect cells using the baculovirus expression system. Half of the protein purified by immunoaffinity chromatography was shown to be N-glycosylated at the same site as the natural IFN-omega 1. The degree of glycosylation was independent of the expression rate. While natural IFN-omega 1 was shown to carry complex-type oligosaccharides [Adolf, G. R., Maurer-Fogy, I., Kalsner, I. & Cantell, K. (1990) J. Biol. Chem. 265, 9290-9295], the insect cell produced protein which was demonstrated by lectin blot, mass spectroscopy and HPLC analysis to contain only the core oligosaccharide. Two different structures, (Man)2(GlcNAc)2[Fuc] and (Man)3(GlcNAc)2[Fuc] were identified. The fucosylation was identified to be (alpha 1-6)-linked to the core saccharide. Sialic acid residues were clearly absent. IFN-omega 1 expressed in S. frugiperda cells was shown to be partially truncated at the C-terminus by nine residues; its antiviral activity when glycosylated was significantly lower than the activity of IFN-omega 1 produced by Sendai-virus-stimulated leukocytes. Circular dichroism and fluorescence spectroscopy did not reveal any structural differences between glycosylated and nonglycosylated IFN-omega 1. This implies the importance of a complex-type glycosylation for the maximal biological activity of human IFN-omega 1.

MeSH terms

  • Animals
  • Baculoviridae / genetics
  • Base Sequence
  • Carbohydrate Sequence
  • Carbohydrates / analysis
  • Cell Line
  • Cells, Cultured
  • Chromatography, High Pressure Liquid
  • Circular Dichroism
  • Cloning, Molecular
  • DNA Primers
  • Electrophoresis, Polyacrylamide Gel
  • Glycosylation
  • Humans
  • Interferon Type I / genetics*
  • Interferon Type I / isolation & purification
  • Interferon Type I / metabolism
  • Mass Spectrometry
  • Molecular Sequence Data
  • Moths
  • N-Acetylneuraminic Acid
  • Protein Conformation
  • Sialic Acids / metabolism*
  • Spectrometry, Fluorescence

Substances

  • Carbohydrates
  • DNA Primers
  • Interferon Type I
  • Sialic Acids
  • interferon omega 1
  • N-Acetylneuraminic Acid