Immunoaffinity purification of an oxidase-activating cytosolic complex from bovine neutrophils

Biochem Biophys Res Commun. 1993 Dec 30;197(3):1296-302. doi: 10.1006/bbrc.1993.2618.

Abstract

An oxidase activating complex from the cytosol of bovine neutrophils was purified by immunoaffinity using a monoclonal antibody specific for the 67 kDa cytosolic factor of oxidase activation (p67) and assayed for production of superoxide O2- in a cell-free system. The complex comprised not only p67, but also the second cytosolic factor of 47 kDa (p47) in equivalent amounts. The p47-p67 complex showed a good oxidase activating potency when added to neutrophil membranes in the presence of GTP-gamma-S and arachidonic acid. A ras-related small G protein could not be immunodetected in the p47-p67 activating complex, indicating that the GTP required for oxidase activation in the cell free system bound to a protein that was either present in catalytic amounts in the cytosolic complex or present in sufficient amount in the membrane fraction.

MeSH terms

  • Animals
  • Blotting, Western
  • Cattle
  • Cell-Free System
  • Chromatography, Affinity
  • Cytosol / enzymology
  • Electrophoresis, Polyacrylamide Gel
  • Molecular Weight
  • NADH, NADPH Oxidoreductases / blood*
  • NADH, NADPH Oxidoreductases / isolation & purification
  • NADPH Oxidases
  • Neutrophils / enzymology*
  • Superoxides / blood

Substances

  • Superoxides
  • NADH, NADPH Oxidoreductases
  • NADPH Oxidases