The (3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium) colorimetric assay for the quantitation of Actinobacillus pleuropneumoniae cytotoxin

Can J Vet Res. 1993 Jul;57(3):159-65.

Abstract

Using swine neutrophils as target cells, two MTT (3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium) colorimetric assay systems, one with and one without phorbol 12-myristate 13-acetate (PMA) stimulation were established for the quantitation of Actinobacillus pleuropneumoniae cytotoxin. The MTT assays were optimized for the number of neutrophils, incubation time, and PMA concentration by a series of experiments. The optimal conditions were 25 x 10(4) cells/well incubated for four hours for the assay system without PMA stimulation, and 12.5 x 10(4) cells/well incubated for two hours for the assay system with PMA stimulation. One culture supernatant of a toxigenic Pasteurella multocida strain and five A. pleuropneumoniae cytotoxin preparations produced from three A. pleuropneumoniae strains were used to test assay reproducibility. Results showed both assays were reproducible with a coefficient of variation ranging from 7.8 to 18% for the assay system without PMA stimulation and from 10.7 to 18.2% for the assay system with PMA stimulation. The PMA-stimulated assay had 40 to 60-fold higher sensitivity than the nonstimulated MTT assay. The MTT assay also was applied to the measurement of neutralizing antibody titers against A. pleuropneumoniae cytotoxin.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Actinobacillus pleuropneumoniae / metabolism*
  • Animals
  • Cells, Cultured
  • Colorimetry
  • Coloring Agents*
  • Cytotoxins / analysis*
  • Cytotoxins / immunology
  • Cytotoxins / toxicity
  • Immune Sera / immunology
  • Neutrophils / drug effects
  • Regression Analysis
  • Reproducibility of Results
  • Swine
  • Tetradecanoylphorbol Acetate
  • Tetrazolium Salts* / metabolism
  • Thiazoles* / metabolism

Substances

  • Coloring Agents
  • Cytotoxins
  • Immune Sera
  • Tetrazolium Salts
  • Thiazoles
  • thiazolyl blue
  • Tetradecanoylphorbol Acetate