A novel constrained reduced-amide inhibitor of HIV-1 protease derived from the sequential incorporation of gamma-turn mimetics into a model substrate

J Med Chem. 1993 Aug 6;36(16):2321-31. doi: 10.1021/jm00068a008.

Abstract

C7 mimetics, designed to lock three amino acid residues of a peptide chain into a gamma-turn conformation, were introduced sequentially between the P3 to P2' positions of a model HIV-1 protease substrate I (resulting in compounds II-IV) to probe its conformational requirements in binding to HIV-1 protease. Of these, compound IIIa with the C7 mimetic replacing Asn-Tyr-Pro, corresponding to the P2 through P1' positions of substrate, was found to be an inhibitor with a Ki of 147 microM. Reduction of the amide bond in the C7 mimetic of IIIa resulted in a novel constrained reduced-amide mimetic VIa with a Ki of 430 nM. This corresponds to over a 300-fold improvement in inhibitory activity over the original C7 mimetic. The inhibitory activity of mimetic VIa was in addition found to be 44-fold better than a similar linear reduced-amide containing inhibitor V. The synthesis of these mimetics are described.

MeSH terms

  • HIV Protease Inhibitors / chemical synthesis*
  • HIV Protease Inhibitors / metabolism
  • Structure-Activity Relationship
  • Sympathomimetics / chemical synthesis*
  • Sympathomimetics / metabolism

Substances

  • HIV Protease Inhibitors
  • Sympathomimetics