Reconstitution of barley photosystem I with modified PSI-C allows identification of domains interacting with PSI-D and PSI-A/B

J Biol Chem. 1996 Apr 12;271(15):8996-9001. doi: 10.1074/jbc.271.15.8996.

Abstract

The PSI-C subunit of photosystem I shows similarity to soluble 2[4Fe-4S] ferredoxins. Alignment analysis clearly shows that PSI-C contains an 8-residue internal loop and a 15-residue C-terminal extension that are absent in the ferredoxins. The remaining residues in PSI-C are likely to be folded in a way similar to the soluble 2[4Fe-4S] ferredoxins. Two modified PSI-C subunits lacking either the 8-residue loop or 10 residues of the C terminus were expressed in Escherichia coli and used to reconstitute a barley P700-FX core prepared to specifically lack PSI-C, PSI-D, and PSI-E. As shown by EPR spectroscopy, the modified proteins carry two [4Fe-4S] clusters with characteristics similar to those of native PSI-C. Western blot analysis of the reconstituted photosystem I complexes showed that the modified PSI-C proteins bind to the P700-FX core. Flash photolysis revealed that in photosystem I complexes reconstituted in the presence of PSI-D with the C-terminally deleted PSI-C, the FA/FB back-reaction was less efficiently restored than with wild-type PSI-C. The loop-deleted PSI-C was even less efficient. We attribute these differences to altered binding properties of the modified proteins. Comparison of reconstitutions performed in the presence and absence of PSI-D shows that the loop-deleted PSI-C is unable to bind without PSI-D, whereas the C-terminally deleted PSI-C binds only weakly with PSI-D. These results imply that the internal loop of PSI-C interacts with the PSI-A/B heterodimer and that the C terminus of PSI-C interacts with PSI-D.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Electron Spin Resonance Spectroscopy
  • Hordeum
  • Iron-Sulfur Proteins / chemistry*
  • Macromolecular Substances
  • Molecular Sequence Data
  • NADP / chemistry
  • Photochemistry
  • Photosynthetic Reaction Center Complex Proteins / chemistry*
  • Photosystem I Protein Complex
  • Plant Proteins / chemistry*
  • Recombinant Proteins
  • Sequence Deletion
  • Structure-Activity Relationship

Substances

  • Iron-Sulfur Proteins
  • Macromolecular Substances
  • Photosynthetic Reaction Center Complex Proteins
  • Photosystem I Protein Complex
  • Plant Proteins
  • Recombinant Proteins
  • NADP