Action on bovine alpha s1-casein of cardosins A and B, aspartic proteinases from the flowers of the cardoon Cynara cardunculus L

Biochim Biophys Acta. 1996 Sep 13;1297(1):83-9. doi: 10.1016/0167-4838(96)00103-3.

Abstract

The cleavage of purified bovine alpha s1-casein separately by cardosin A and cardosin B, two distinct milk-clotting aspartic proteinases (APs) present in the stigmas of the plant Cynara cardunculus L., was studied. Casein digestion peptides were separated either by SDS-PAGE or by reverse-phase HPLC, and their N-terminal amino acid sequences were subsequently determined by automated Edman degradation, thus identifying the cleavage sites. Results showed that both enzymes exert a similar but distinct action on bovine alpha s1-casein. In common they have the preference for the bond Phe23-Phe24, and the cleavage of Trp164-Tyr165 and Phe153-Tyr154. Cardosin A also cleaves the bond Tyr165-Tyr166, whereas Cardosin B cleaves an extra type of bond, Phe150-Arg151, revealing a slightly broader specificity. A model for the action of both enzymes on bovine alpha s1-casein is proposed and discussed. In comparison with the reported action of chymosin on bovine alpha s1-casein, both cardosins proved to have a broader specificity towards this particular substrate due to a higher ability to cleave bonds between residues with large hydrophobic side-chains.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Arginine / metabolism
  • Aspartic Acid Endopeptidases / isolation & purification
  • Aspartic Acid Endopeptidases / metabolism*
  • Caseins / metabolism*
  • Cattle
  • Molecular Weight
  • Peptide Fragments / analysis
  • Peptide Fragments / chemistry
  • Phenylalanine / metabolism
  • Plant Proteins / isolation & purification
  • Plant Proteins / metabolism*
  • Plants / enzymology*
  • Sequence Analysis
  • Substrate Specificity
  • Tryptophan / metabolism
  • Tyrosine / metabolism

Substances

  • Caseins
  • Peptide Fragments
  • Plant Proteins
  • Tyrosine
  • Phenylalanine
  • Tryptophan
  • Arginine
  • Aspartic Acid Endopeptidases
  • aspartic proteinases, Cynara cardunculus