Highly sensitive qualitative and quantitative detection of reverse transcriptase activity: optimization, validation, and comparative analysis with other detection systems

J Virol Methods. 1996 Sep;61(1-2):135-43. doi: 10.1016/0166-0934(96)02078-2.

Abstract

An ultra-sensitive assay for reverse transcriptase (RT) activity called Amp-RT has been developed. An in vitro transcribed heteropolymeric RNA sequence was used as a template, and polymerase chain reaction (PCR) amplification with Southern-blot hybridization served as a detection system for the cDNA product of the reaction. Titration of Mg2+ and Mn2+ concentrations using the human immunodeficiency virus type 1 (HIV-1) and the human T lymphotropic virus type 1 (HTLV-I), respectively, showed optimal assay reactivity for both viruses at 2-20 mM of Mg2+. Analysis of density banded HIV-1 showed that the peak RT activity of the assay was associated with the fractions consistent with retrovirus particles. The sensitivity of Amp-RT was also compared with that of three conventional RT assays by using seven different retroviruses including HIV-1, simian immunodeficiency virus (SIV), caprine arthritis-encephalitis virus (CAEV), HTLV-I and HTLV-II, simian retrovirus type 2 (SRV-2), and gibbon ape leukemia virus (GALV). HTLV-I, HTLV-II, and GALV could not be detected by the three conventional RT assays. Amp-RT was able to detect all these viruses in 10(1)-10(3)-fold dilutions. Similarly, Amp-RT was found to be 10(3)-10(6)-fold more sensitive than the other RT assays in detecting HIV-1, SIV< or CAEV. Culture supernatants from uninfected cell lines were all Amp-RT negative. A quantitative Amp-RT assay was also developed by using recombinant HIV-1 RT and signal quantitation. The assay was found to have a 5 log linear range, and therefore, provides a useful tool for quantitating RT and retroviruses. Amp-RT offers a sensitive generic tool for the qualitative and quantitative detection of known and unknown retroviruses.

Publication types

  • Comparative Study

MeSH terms

  • Animals
  • Blotting, Southern / methods*
  • Centrifugation, Density Gradient
  • Enzyme-Linked Immunosorbent Assay
  • HIV Reverse Transcriptase / genetics
  • HIV-1 / enzymology
  • Humans
  • Magnesium
  • Manganese
  • Polymerase Chain Reaction / methods*
  • RNA, Viral / analysis*
  • RNA-Directed DNA Polymerase / genetics*
  • Retroviridae / isolation & purification*
  • Retroviridae Proteins / genetics*
  • Sensitivity and Specificity
  • Sucrose
  • Tumor Cells, Cultured

Substances

  • RNA, Viral
  • Retroviridae Proteins
  • Manganese
  • Sucrose
  • HIV Reverse Transcriptase
  • RNA-Directed DNA Polymerase
  • Magnesium