Rational engineering of activity and specificity in a serine protease

Nat Biotechnol. 1997 Feb;15(2):146-9. doi: 10.1038/nbt0297-146.

Abstract

The discovery of the Na(+)-dependent allosteric regulation in serine proteases makes it possible to control catalytic activity and specificity in this class of enzymes in a way never considered before. We demonstrate that rational site-directed mutagenesis of residues controlling Na+ binding can profoundly after the properties of a serine protease. By suppressing Na+ binding to thrombin, we shift the balance between procoagulant and anticoagulant activities of the enzyme. Those mutants, compared to wild-type, have reduced specificity toward fibrinogen, but enhanced or slightly reduced specificity toward protein C. Because this engineering strategy targets a fundamental regulatory mechanism, it is amenable of extension to other enzymes of biological and pharmacological importance.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amino Acid Sequence
  • Anticoagulants
  • Binding Sites
  • Coagulants
  • Fibrinogen / metabolism
  • Humans
  • Kinetics
  • Models, Molecular
  • Mutagenesis, Site-Directed
  • Point Mutation
  • Polymerase Chain Reaction
  • Protein C / metabolism
  • Protein Conformation
  • Protein Engineering / methods
  • Recombinant Proteins / biosynthesis
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / metabolism*
  • Sodium / metabolism
  • Substrate Specificity
  • Thrombin / biosynthesis
  • Thrombin / chemistry
  • Thrombin / metabolism*
  • Thrombomodulin / metabolism

Substances

  • Anticoagulants
  • Coagulants
  • Protein C
  • Recombinant Proteins
  • Thrombomodulin
  • Fibrinogen
  • Sodium
  • Thrombin