Functional and idling rotatory motion within F1-ATPase

Proc Natl Acad Sci U S A. 1997 Apr 29;94(9):4401-5. doi: 10.1073/pnas.94.9.4401.

Abstract

ATP synthase mediates proton flow through its membrane portion, F0, which drives the synthesis of ATP in its headpiece, F1. The F1-portion contains a hexagonal array of three subunits alpha and three beta encircling a central subunit gamma, that in turn interacts with a smaller epsilon and with F0. Recently we reported that the application of polarized absorption recovery after photobleaching showed the ATP-driven rotation of gamma over at least two, if not three, beta. Here we extend probes of such rotation aided by a new theory for assessing continuous versus stepped, Brownian versus unidirectional molecular motion. The observed relaxation of the absorption anisotropy is fully compatible with a unidirectional and stepping rotation of gamma over three equidistantly spaced angular positions in the hexagon formed by the alternating subunits alpha and beta. The results strongly support a rotational catalysis with equal participation of all three catalytic sites. In addition we report a limited rotation of gamma without added nucleotides, perhaps idling and of Brownian nature, that covers only a narrow angular domain.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Triphosphate / metabolism*
  • Adenylyl Imidodiphosphate / metabolism
  • Anisotropy
  • Biophysics / instrumentation
  • Biophysics / methods*
  • Chloroplasts / enzymology
  • Enzymes, Immobilized / physiology
  • Eosine Yellowish-(YS)
  • Lasers
  • Models, Molecular
  • Models, Theoretical
  • Molecular Probes
  • Motion
  • Movement / physiology*
  • Proton-Translocating ATPases / physiology*
  • Proton-Translocating ATPases / radiation effects
  • Spinacia oleracea / enzymology

Substances

  • Enzymes, Immobilized
  • Molecular Probes
  • Adenylyl Imidodiphosphate
  • Adenosine Triphosphate
  • Proton-Translocating ATPases
  • Eosine Yellowish-(YS)