Epitope tagging and immunoreactivity of the human angiotensin II type 1 receptor

Can J Physiol Pharmacol. 1997 Jun;75(6):690-5.

Abstract

Structural analysis of G-protein-coupled receptors has largely been limited to photoaffinity labeling and site-directed mutagenesis. This is primarily due to the difficulty in the production of antibodies against this class of receptors. We were therefore interested in tagging the amino-terminal side of the human angiotensin II (AngII) type 1 receptor (AT1) with the FLAG epitope DYKDDDDK. Competitive binding experiments with [125I][Sar1,Ile8]AngII revealed that stably transfected Chinese hamster ovary (CHO) cells express 37,300 hAT1-FLAG receptors/cell with a high affinity of 0.53 nM, comparable with that of the wild-type hAT1. After photolabeling and solubilization, a significant proportion of hAT1-FLAG specifically immunoprecipitated with anti-FLAG M5 and M2 antibodies. The immunoprecipitated receptor comigrated on SDS-PAGE with photolabeled wild-type hAT1. Immunofluorescence studies by FACS scan analysis revealed that 11.9% of CHO cells expressing hAT1-FLAG receptor significantly increased their fluorescence level as a result of M5 specific reactivity. Western blot analysis failed to show any specific interaction between M5 antibody and denatured hAT1-FLAG receptor. These results demonstrate the efficiency of the epitope tagging approach for specific immunoreactivity against AT1 receptor. Appropriate refinements of this approach could improve the level of immunoreactivity.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Affinity Labels
  • Animals
  • Antibodies / immunology
  • Antibody Specificity
  • CHO Cells / metabolism
  • CHO Cells / physiology
  • Cricetinae
  • DNA, Complementary / genetics
  • DNA, Complementary / metabolism
  • Epitopes / immunology*
  • Epitopes / metabolism
  • Flow Cytometry
  • Humans
  • Mutagenesis, Site-Directed
  • Oligopeptides
  • Peptides / immunology*
  • Peptides / metabolism
  • Receptor, Angiotensin, Type 1
  • Receptor, Angiotensin, Type 2
  • Receptors, Angiotensin / biosynthesis
  • Receptors, Angiotensin / genetics
  • Receptors, Angiotensin / immunology*
  • Recombinant Fusion Proteins / biosynthesis
  • Recombinant Fusion Proteins / genetics
  • Recombinant Fusion Proteins / immunology

Substances

  • Affinity Labels
  • Antibodies
  • DNA, Complementary
  • Epitopes
  • Oligopeptides
  • Peptides
  • Receptor, Angiotensin, Type 1
  • Receptor, Angiotensin, Type 2
  • Receptors, Angiotensin
  • Recombinant Fusion Proteins
  • FLAG peptide