14-3-3zeta binds a phosphorylated Raf peptide and an unphosphorylated peptide via its conserved amphipathic groove

J Biol Chem. 1998 Jun 26;273(26):16305-10. doi: 10.1074/jbc.273.26.16305.

Abstract

14-3-3 proteins bind a variety of molecules involved in signal transduction, cell cycle regulation and apoptosis. 14-3-3 binds ligands such as Raf-1 kinase and Bad by recognizing the phosphorylated consensus motif, RSXpSXP, but must bind unphosphorylated ligands, such as glycoprotein Ib and Pseudomonas aeruginosa exoenzyme S, via a different motif. Here we report the crystal structures of the zeta isoform of 14-3-3 in complex with two peptide ligands: a Raf-derived phosphopeptide (pS-Raf-259, LSQRQRSTpSTPNVHMV) and an unphosphorylated peptide derived from phage display (R18, PHCVPRDLSWLDLEANMCLP) that inhibits binding of exoenzyme S and Raf-1. The two peptides bind within a conserved amphipathic groove on the surface of 14-3-3 at overlapping but distinct sites. The phosphoserine of pS-Raf-259 engages a cluster of basic residues (Lys49, Arg56, Arg60, and Arg127), whereas R18 binds via the amphipathic sequence, WLDLE, with its two acidic groups coordinating the same basic cluster. 14-3-3 is dimeric, and its two peptide-binding grooves are arranged in an antiparallel fashion, 30 A apart. The ability of each groove to bind different peptide motifs suggests how 14-3-3 can act in signal transduction by inducing either homodimer or heterodimer formation in its target proteins.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • 14-3-3 Proteins
  • ADP Ribose Transferases*
  • Amino Acid Sequence
  • Animals
  • Bacterial Toxins*
  • Binding Sites
  • Carrier Proteins / metabolism
  • Crystallography, X-Ray
  • Dimerization
  • Enzyme Inhibitors / metabolism*
  • Models, Molecular
  • Molecular Sequence Data
  • Phosphorylation
  • Phosphoserine / metabolism
  • Platelet Glycoprotein GPIb-IX Complex / metabolism
  • Poly(ADP-ribose) Polymerases / metabolism
  • Protein Conformation
  • Proteins / genetics
  • Proteins / metabolism*
  • Proto-Oncogene Proteins c-raf / metabolism*
  • Pseudomonas aeruginosa
  • Signal Transduction
  • Tyrosine 3-Monooxygenase*
  • Xenopus laevis
  • bcl-Associated Death Protein

Substances

  • 14-3-3 Proteins
  • Bacterial Toxins
  • Carrier Proteins
  • Enzyme Inhibitors
  • Platelet Glycoprotein GPIb-IX Complex
  • Proteins
  • bcl-Associated Death Protein
  • Phosphoserine
  • Tyrosine 3-Monooxygenase
  • ADP Ribose Transferases
  • Poly(ADP-ribose) Polymerases
  • exoenzyme S
  • Proto-Oncogene Proteins c-raf

Associated data

  • PDB/1A37
  • PDB/1A38
  • PDB/1A40