Stability of 2'-deoxyxanthosine in DNA

Nucleic Acids Res. 2003 Feb 1;31(3):1045-51. doi: 10.1093/nar/gkg177.

Abstract

The deamination of nucleobases in DNA occurs by a variety of mechanisms and results in the formation of hypoxanthine from adenine, uracil from cytosine, and xanthine and oxanine from guanine. 2'-Deoxyxanthosine (dX) has been assumed to be an unstable lesion in cells, yet no study has been performed under biological conditions. We now report that dX is a relatively stable lesion at pH 7, 37 degrees C and 110 mM ionic strength, with a half-life (t(1/2)) of 2.4 years in double-stranded DNA. The stability of dX as a 2'-deoxynucleoside (t(1/2) = 3.7 min at pH 2; 1104 h at pH 6) was increased substantially upon incorporation into a single-stranded oligodeoxynucleotide, in which the half-life of dX at different pH values was found to range from 7.7 h at pH 2 to 17 700 h at pH 7. Incorporation of dX into a double-stranded oligodeoxynucleotide resulted in a statistically insignificant increase in the half-life to 20 900 h at pH 7. Data for the pH dependence of the stability of dX in single-stranded DNA were used to determine the rate constants for the acid-catalyzed (2.6 x 10(-5) x s(-1)) and pH-independent (1.4 x 10(-8) x s(-1)) depurination reactions for dX as well as the dissociation constant for the N7 position of dX (6.1 x 10(-4) M). We conclude that dX is a relatively stable lesion that could play a role in deamination-induced mutagenesis.

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Amination
  • DNA / chemistry*
  • Deoxyribonucleosides / chemistry*
  • Deoxyribonucleosides / metabolism
  • Half-Life
  • Hydrogen-Ion Concentration
  • Kinetics
  • Models, Chemical
  • Oligodeoxyribonucleotides / chemistry

Substances

  • Deoxyribonucleosides
  • Oligodeoxyribonucleotides
  • 2'-deoxyxanthosine
  • DNA