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10 pages, 1440 KiB  
Article
Photothermal Effect of 970 nm Diode Laser Irradiation on Enterococcus faecalis Biofilms in Single-Rooted Teeth Ex Vivo
by Soraya Tanner, Anna Thibault, Julian Grégoire Leprince and Serge Bouillaguet
Dent. J. 2024, 12(10), 308; https://doi.org/10.3390/dj12100308 - 27 Sep 2024
Abstract
Objective: The aim of this study was to evaluate the photothermal effect of a 970 nm diode laser on Enterococcus faecalis biofilms. Methods: 72 extracted human single-rooted teeth were prepared, sterilized, and inoculated with Enterococcus faecalis to establish a two-week-old biofilm. [...] Read more.
Objective: The aim of this study was to evaluate the photothermal effect of a 970 nm diode laser on Enterococcus faecalis biofilms. Methods: 72 extracted human single-rooted teeth were prepared, sterilized, and inoculated with Enterococcus faecalis to establish a two-week-old biofilm. The specimens were divided into six groups (n = 12): Group 1 (G1)—negative control (PBS—no laser), Group 2 (G2)—positive control (1% NaOCl rinse—no laser), Group 3 (G3)—a 970 nm laser in 1.5 W pulse mode, Group 4 (G4)—a 970 nm laser in 2 W pulse mode, Group 5 (G5)—a 970 nm laser in 1.5 W continuous mode, Group 6 (G6)—a 970 nm laser in 2 W continuous mode. Bacterial viability was evaluated using the LIVE/DEAD BacLight kit and analyzed by flow cytometry (FCM). Temperature changes on the root surface during irradiation were analyzed using a K-type thermocouple. Data were statistically analyzed using one-way ANOVA and Tukey’s multiple comparison test (α = 0.05). Results: Bacterial viability was significantly reduced after laser irradiation in continuous mode using 1.5 W (21% of live bacteria) and 2 W (14% of live bacteria). When the pulsed mode was applied, the reduction in bacterial viability was less, with a mean survival of 53% (1.5 PF, whereas 29% of bacteria survived after 2 W irradiation). Conclusions: The 970 nm diode laser at 2 W continuous mode effectively reduced the viability of E. faecalis biofilms in root canals without causing unacceptable temperature rises at the root surface. Full article
(This article belongs to the Special Issue Endodontics and Restorative Sciences: 2nd Edition)
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27 pages, 2408 KiB  
Article
Study of the Thermomechanical Behavior of Single-Crystal and Polycrystal Copper
by Sudip Kunda, Noah J. Schmelzer, Akhilesh Pedgaonkar, Jack E. Rees, Samuel D. Dunham, Charles K. C. Lieou, Justin C. M. Langbaum and Curt A. Bronkhorst
Metals 2024, 14(9), 1086; https://doi.org/10.3390/met14091086 - 22 Sep 2024
Abstract
This research paper presents an experimental, theoretical, and numerical study of the thermomechanical behavior of single-crystal and polycrystal copper under uniaxial stress compression loading at varying rates of deformation. The thermomechanical theory is based on a thermodynamically consistent framework for single-crystal face-centered cubic [...] Read more.
This research paper presents an experimental, theoretical, and numerical study of the thermomechanical behavior of single-crystal and polycrystal copper under uniaxial stress compression loading at varying rates of deformation. The thermomechanical theory is based on a thermodynamically consistent framework for single-crystal face-centered cubic metals, and assumes that all plastic power is partitioned between stored energy due to dislocation structure evolution (configurational) and thermal (kinetic vibrational) energy. An expression for the Taylor–Quinney factor is proposed, which is a simple function of effective temperature and is allowed by second-law restrictions. This single-crystal model is used for the study of single- and polycrystal copper. New polycrystal thermomechanical experimental results are presented at varying strain rates. The temperature evolution on the surface of the polycrystal samples is measured using mounted thermocouples. Thermomechanical numerical single- and polycrystal simulations were performed for all experimental conditions ranging between 103 and 5 × 103 s1. A Taylor homogenization model is used to represent polycrystal behavior. The numerical simulations of all conditions compare reasonable well with experimental results for both stress and temperature evolution. Given our lack of understanding of the mechanisms responsible for the coupling of dislocation glide and atomic vibration, this implies that the proposed theory is a reasonably accurate approximation of the single-crystal thermomechanics. Full article
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14 pages, 3358 KiB  
Article
Accurately Measuring the Infrared Spectral Emissivity of Inconel 601, Inconel 625, and Inconel 718 Alloys during the Oxidation Process
by Longfei Li, Fayu Wang, Jiaying Gao, Kun Yu, Lan Wang and Yufang Liu
Sensors 2024, 24(18), 5906; https://doi.org/10.3390/s24185906 - 11 Sep 2024
Abstract
Accurate measurement of the infrared spectral emissivity of nickel-based alloys is significant for applications in aerospace. The low thermal conductivity of these alloys limits the accuracy of direct emissivity measurement, especially during the oxidation process. To improve measurement accuracy, a surface temperature correction [...] Read more.
Accurate measurement of the infrared spectral emissivity of nickel-based alloys is significant for applications in aerospace. The low thermal conductivity of these alloys limits the accuracy of direct emissivity measurement, especially during the oxidation process. To improve measurement accuracy, a surface temperature correction method based on two thermocouples was proposed to eliminate the effect of thermal conductivity changes on emissivity measurement. By using this method, the infrared spectral emissivity of Inconel 601, Inconel 625, and Inconel 718 alloys was accurately measured during the oxidation process, with a temperature range of 673–873 K, a wavelength range of 3–20 μm, and a zenith angle range of 0–80°. The results show that the emissivity of the three alloys is similar in value and variation law; the emissivity of Inconel 718 is slightly less than that of Inconel 601 and Inconel 625; and the spectral emissivity of the three alloys strongly increases in the first hour, whereafter it grows gradually with the increase in oxidation time. Finally, Inconel 601 has a lower emissivity growth rate, which illustrates that it possesses stronger oxidation resistance and thermal stability. The maximum relative uncertainty of the emissivity measurement of the three alloys does not exceed 2.6%, except for the atmospheric absorption wavebands. Full article
(This article belongs to the Section Optical Sensors)
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15 pages, 7126 KiB  
Article
Study of Heat Distribution in Railway Switch Using Resistive Heater in Cold Climate Conditions
by Arefeh Lotfi, Adeel Yousuf and Muhammad Shakeel Virk
Appl. Sci. 2024, 14(18), 8151; https://doi.org/10.3390/app14188151 - 11 Sep 2024
Abstract
The railway is an essential source of logistics and transportation in cold regions, but low temperatures and icing can be challenging for uninterrupted railway operations in these regions. Icing on railway switches is a safety hazard, and presently, one of the industry’s adaptive [...] Read more.
The railway is an essential source of logistics and transportation in cold regions, but low temperatures and icing can be challenging for uninterrupted railway operations in these regions. Icing on railway switches is a safety hazard, and presently, one of the industry’s adaptive approaches for ice mitigation is the use of resistive heaters. This method is efficient but consumes a great amount of electricity, leading to high financial costs in terms of the operation and maintenance of railway tracks in ice-prone regions. In this paper, a study is carried out using experiments and computational simulations to analyze the heat distribution in a cross-section of a rail at below-freezing temperatures. Experiments are performed in a cold room using an actual rail switch, thermocouples, and infrared imaging, while numerical analyses are carried out using a MATLAB-based analytical model to simulate the heat transfer, considering a section of stock rail and a heating element. Results show a considerable loss of heat from the heater to the surroundings of the rail, especially towards the ground ballast. Numerical simulation results provide a good insight into heat transfer along railway sections, and results are validated with experiments, where a good agreement is found. This study provides a good base for further optimization of resistive heating operations for ice mitigation along railway switches. Full article
(This article belongs to the Special Issue Fluid Flow and Heat Transfer: Latest Advances and Prospects)
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14 pages, 3889 KiB  
Article
Heat Generation during Dental Implant Bed Preparation Using Surgical Guides with and without Internal Irrigation Channels Evaluated on Standardized Models of the Alveolar Bone
by Robert-Angelo Tuce, Monica Neagu, Vasile Pupăzan, Adrian Neagu and Stelian Arjoca
Appl. Sci. 2024, 14(17), 8051; https://doi.org/10.3390/app14178051 - 9 Sep 2024
Abstract
Dental implant bed preparation involves surgical drilling. Heat generated in this process can cause a temperature elevation beyond the bone damage limit (10 °C), affecting the osseointegration of the implant. Surgical templates ensure accurate implant placement, but they limit the access of the [...] Read more.
Dental implant bed preparation involves surgical drilling. Heat generated in this process can cause a temperature elevation beyond the bone damage limit (10 °C), affecting the osseointegration of the implant. Surgical templates ensure accurate implant placement, but they limit the access of the irrigation fluid. This study evaluated the hypothesis that surgical guides with internal cooling prevent bone heating more effectively than classical guides. To eliminate biological variability, this study was conducted on artificial bone pieces that mimic the bone density of the human mandible. We created a surgical template that incorporated four pairs of guides—one classical (CLA) and one with internal cooling (INT) in each pair. For each specimen, we randomly selected the type of surgical guide to start with and performed four osteotomies with a 2.7 mm-diameter drill; then, we widened each hole with a 3.3 mm drill and finalized it with a 3.7 mm drill. The temperature was recorded by thermocouples placed at 0.8 mm from the prospective edge of the final osteotomy. In 168 measurements (12 osteotomies on 14 specimens) conducted for each type of surgical guide, the mean temperature rise was 7.2 ± 4.9 °C (mean ± standard deviation) for CLA and 5.0 ± 3.8 °C for INT. The mean differences between temperature elevations were 1.5 °C, 2.1 °C, and 3.0 °C for the first, second, and third drill, and they were statistically significant: the p-values of Student’s t-test were 0.004, 0.01, and 0.001, respectively. Although the mean temperatures remained safe, temperature rises exceeded 10 °C in 23.8% (9.5%) of the osteotomies performed in the presence of CLA (INT). Taken together, our results suggest that surgical guides with internal cooling ensure a significant drop in the temperature rise caused by implant site drilling. Full article
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12 pages, 4615 KiB  
Article
A Study on Miniaturized In-Situ Self-Calibrated Thermometers Based on Ga and Ga-Zn Fixed Points
by Haiying Huang, Wenlu Cai, Yongjian Mao, Kun Wan, Yong Wen, Yuqiang Han, Qiang Zhang, Rong Zhang and Xing Zheng
Sensors 2024, 24(17), 5744; https://doi.org/10.3390/s24175744 - 4 Sep 2024
Viewed by 154
Abstract
In order to ensure the reliability and accuracy of long-term temperature measurement where the thermometers are discommodious or even impossible to access for conventional periodical calibration, a study on miniaturized in-situ self-calibrated (MISSC) thermometers based on Ga and Ga-Zn fixed points was conducted [...] Read more.
In order to ensure the reliability and accuracy of long-term temperature measurement where the thermometers are discommodious or even impossible to access for conventional periodical calibration, a study on miniaturized in-situ self-calibrated (MISSC) thermometers based on Ga and Ga-Zn fixed points was conducted using temperature scale transfer technology. One MISSC thermometer consists of three parts: the first is the fixed-points hardware, including a container with two cells separately filled with Ga and Ga-Zn; the second is the temperature sensing hardware, made of a Type T thermocouple; the third is the mini-power heating hardware, made of a film resistance. The measurement and calibration (M&C) system comprises a temperature measurement and data processing subsystem and a mini-power heating control subsystem. Then, an in-situ self-calibration can be carried out by mini-power heating from a room temperature of about 20 °C, and then by comparison between the measured phase transition plateau results and the standard fixed-points, i.e., Ga fixed point (about 29.76 °C) and Ga-Zn fixed point (about 25.20 °C). A series of experiments were performed, and the results show that: (1) both the proposed hardware design and the self-calibration method are feasible, and (2) the Φ16 mm × 25 mm MISSC thermometer is found to be the most miniaturized one that can realize reliable self-calibration in this study. Full article
(This article belongs to the Section Physical Sensors)
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18 pages, 6151 KiB  
Article
Enhancing the Fire Resistance of Ablative Materials: Role of the Polymeric Matrix and Silicon Carbide Reinforcement
by Juana Abenojar, Sara López de Armentia and Miguel Angel Martínez
Polymers 2024, 16(17), 2454; https://doi.org/10.3390/polym16172454 - 29 Aug 2024
Viewed by 301
Abstract
The primary characteristic of ablative materials is their fire resistance. This study explored the development of cost-effective ablative materials formed into application-specific shapes by using a polymer matrix reinforced with ceramic powder. A thermoplastic (polypropylene; PP) and a thermoset (polyester; UPE) matrix were [...] Read more.
The primary characteristic of ablative materials is their fire resistance. This study explored the development of cost-effective ablative materials formed into application-specific shapes by using a polymer matrix reinforced with ceramic powder. A thermoplastic (polypropylene; PP) and a thermoset (polyester; UPE) matrix were used to manufacture ablative materials with 50 wt% silicon carbide (SiC) particles. The reference composites (50 wt% SiC) were compared to those with 1 and 3 wt% short glass fibers (0.5 mm length) and to composites using a 1 and 3 wt% glass fiber mesh. Fire resistance was tested using a butane flame (900 °C) and by measuring the transmitted heat with a thermocouple. Results showed that the type of polymer matrix (PP or UPE) did not influence fire resistance. Composites with short glass fibers had a fire-resistance time of 100 s, while those with glass fiber mesh tripled this resistance time. The novelty of this work lies in the exploration of a specific type of material with unique percentages of SiC not previously studied. The aim is to develop a low-cost coating for industrial warehouses that has improved fire-protective properties, maintains lower temperatures, and enhances the wear and impact resistance. Full article
(This article belongs to the Special Issue Flame-Retardant Polymer Composites II)
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20 pages, 4918 KiB  
Article
Influence of Extrusion Parameters on the Mechanical Properties of Slow Crystallizing Carbon Fiber-Reinforced PAEK in Large Format Additive Manufacturing
by Patrick Consul, Matthias Feuchtgruber, Bernhard Bauer and Klaus Drechsler
Polymers 2024, 16(16), 2364; https://doi.org/10.3390/polym16162364 - 21 Aug 2024
Viewed by 410
Abstract
Additive Manufacturing (AM) enables the automated production of complex geometries with low waste and lead time, notably through Material Extrusion (MEX). This study explores Large Format Additive Manufacturing (LFAM) with carbon fiber-reinforced polyaryletherketones (PAEK), particularly a slow crystallizing grade by Victrex. The research [...] Read more.
Additive Manufacturing (AM) enables the automated production of complex geometries with low waste and lead time, notably through Material Extrusion (MEX). This study explores Large Format Additive Manufacturing (LFAM) with carbon fiber-reinforced polyaryletherketones (PAEK), particularly a slow crystallizing grade by Victrex. The research investigates how extrusion parameters affect the mechanical properties of the printed parts. Key parameters include line width, layer height, layer time, and extrusion temperature, analyzed through a series of controlled experiments. Thermal history during printing, including cooling rates and substrate temperatures, was monitored using thermocouples and infrared cameras. The crystallization behavior of PAEK was replicated in a Differential Scanning Calorimetry (DSC) setup. Mechanical properties were evaluated using three-point bending tests to analyze the impact of thermal conditions at the deposition interface on interlayer bonding and overall part strength. The study suggests aggregated metrics, enthalpy deposition rate and shear rate under the nozzle, that should be maximized to enhance mechanical performance. The findings show that the common practice of setting fixed layer times falls short of ensuring repeatable part quality. Full article
(This article belongs to the Topic Advanced Composites Manufacturing and Plastics Processing)
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30 pages, 13628 KiB  
Article
Sensor-Enhanced Thick Laminated Composite Beams: Manufacturing, Testing, and Numerical Analysis
by Mustafa Basaran, Halit Suleyman Turkmen and Mehmet Yildiz
Sensors 2024, 24(16), 5366; https://doi.org/10.3390/s24165366 - 20 Aug 2024
Viewed by 397
Abstract
This study investigates the manufacturing, testing, and analysis of ultra-thick laminated polymer matrix composite (PMC) beams with the aim of developing high-performance PMC leaf springs for automotive applications. An innovative aspect of this study is the integration of Fiber Bragg Grating (FBG) sensors [...] Read more.
This study investigates the manufacturing, testing, and analysis of ultra-thick laminated polymer matrix composite (PMC) beams with the aim of developing high-performance PMC leaf springs for automotive applications. An innovative aspect of this study is the integration of Fiber Bragg Grating (FBG) sensors and thermocouples (TCs) to monitor residual strain and exothermic reactions in composite structures during curing and post-curing manufacturing cycles. Additionally, the Calibration Coefficients (CCs) are calculated using Strain Gauge measurement results under static three-point bending tests. A major part of the study focuses on developing a properly correlated Finite Element (FE) model with large deflection (LD) effects using geometrical nonlinear analysis (GNA) to understand the deformation behavior of ultra thick composite beam (ComBeam) samples, advancing the understanding of large deformation behavior and filling critical research gaps in composite materials. This model will help assess the internal strain distribution, which is verified by correlating data from FBG sensors, Strain Gauges (SGs), and FE analysis. In addition, this research focuses on the application of FBG sensors in structural health monitoring (SHM) in fatigue tests under three-point bending with the support of load-deflection sensors: a new approach for composites at this scale. This study revealed that the fatigue performance of ComBeam samples drastically decreased with increasing displacement ranges, even at the same maximum level, underscoring the potential of FBG sensors to enhance SHM capabilities linked to smart maintenance. Full article
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13 pages, 3373 KiB  
Article
Performance Study of F-P Pressure Sensor Based on Three-Wavelength Demodulation: High-Temperature, High-Pressure, and High-Dynamic Measurements
by Maocheng Guo, Qi Zhang, Hongtian Zhu, Rui Liang, Yongqiu Zheng, Xiang Zhu, Enbo Wang, Zhaoyi Li, Chenyang Xue and Zhenyin Hai
Sensors 2024, 24(16), 5313; https://doi.org/10.3390/s24165313 - 16 Aug 2024
Viewed by 314
Abstract
F-P (Fabry–Perot) pressure sensors have a wide range of potential applications in high-temperature, high-pressure, and high-dynamic environments. However, existing demodulation methods commonly rely on spectrometers, which limits their application to high-frequency pressure signal acquisition. To solve this problem, this study developed a self-compensated, [...] Read more.
F-P (Fabry–Perot) pressure sensors have a wide range of potential applications in high-temperature, high-pressure, and high-dynamic environments. However, existing demodulation methods commonly rely on spectrometers, which limits their application to high-frequency pressure signal acquisition. To solve this problem, this study developed a self-compensated, three-wavelength demodulation system composite with an F-P pressure sensor and a thermocouple to construct a comprehensive sensing system. The system produces accurate pressure measurements in high-temperature, high-pressure, and high-dynamic environments. In static testing at room temperature, the sensing system shows excellent linearity, and the pressure sensitivity is 158.48 nm/MPa. In high-temperature testing, the sensing system maintains high linearity in the range of 100 °C to 700 °C, with a maximum pressure-indication error of about 0.13 MPa (0~5 MPa). In dynamic testing, the sensor exhibits good response characteristics at 1000 Hz and 5000 Hz sinusoidal pressure frequencies, with a signal-to-noise ratio (SNR) greater than 37 dB and 45 dB, respectively. These results indicate that the sensing system proposed in this study has significant competitive advantages in the field of high-temperature, high-speed, and high-precision pressure measurements and provides an important experimental basis and theoretical support for technological progress in related fields. Full article
(This article belongs to the Section Physical Sensors)
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11 pages, 2181 KiB  
Article
Simulating Error Due to Acquired Thermoelectric Inhomogeneity
by Zida Li and Jingliang Chen
Sensors 2024, 24(16), 5256; https://doi.org/10.3390/s24165256 - 14 Aug 2024
Viewed by 286
Abstract
The best method to prevent error due to inhomogeneity is to use a new thermocouple design—the thermocouple with controlled temperature field (TCTF). It uses the auxiliary furnace to control the temperature field along its legs. Such a design allows setting and maintaining the [...] Read more.
The best method to prevent error due to inhomogeneity is to use a new thermocouple design—the thermocouple with controlled temperature field (TCTF). It uses the auxiliary furnace to control the temperature field along its legs. Such a design allows setting and maintaining the temperature field along the thermocouple (TC) legs for the sensor. Error due to inhomogeneity of TCs cannot appear in a stable temperature field. However, the auxiliary furnace and TCs, to control the temperature field, have errors, so the temperature field along the main TC is maintained with some error. This leads to residual error due to acquired inhomogeneity of the TCTF. We constructed the mathematical models to fit the experimental data of error due to drift for the type K TC. The authors used the constructed models to study error due to inhomogeneity of the TCTF and the conventional type K TC under considerable changes in temperature field. The main results of modelling are as follows: (i) if the changes in temperature field exceed 7 °C, error due to inhomogeneity of the TCTF is lesser than that of the conventional TC; (ii) the maximum error due to inhomogeneity of the conventional type K TC is 10.75 °C; (iii) the maximum error due to inhomogeneity of the TCTF is below 0.2 °C. Full article
(This article belongs to the Section Industrial Sensors)
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14 pages, 3434 KiB  
Article
Metal-Plated Connections in Sustainable Lightweight Construction: A Weak Link in Fire Conditions?
by Michael Kubicki and Haejun Park
Sustainability 2024, 16(16), 6923; https://doi.org/10.3390/su16166923 - 13 Aug 2024
Viewed by 576
Abstract
Lightweight engineered trusses support sustainable construction with the benefits of mass production and fast construction at lower costs. However, the truss system has raised concerns due to premature failure in fire conditions. This study investigates the effect of a thin soot layer on [...] Read more.
Lightweight engineered trusses support sustainable construction with the benefits of mass production and fast construction at lower costs. However, the truss system has raised concerns due to premature failure in fire conditions. This study investigates the effect of a thin soot layer on the surface of the gusset plate and the teeth of the gusset plate on the temperature development within lightweight wood specimens in fire conditions. A 10 cm long, 8.9 cm wide, and 3.8 cm thick dimensional lumber (often called 2 by 4) partially covered by a gusset plate was exposed to a constant incident radiant heat flux. A total of 12 experiments were conducted with four different configurations, bare gusset plates with and without teeth and soot-coated gusset plates with and without teeth, at three different external radiative heat fluxes of 10, 15, and 20 kW/m2. The exposure durations were set to be 60, 40, and 30 min, respectively, to allow the total applied amount of radiant energy for each specimen to be identical. Three thermocouples were installed at a depth of 13 mm from the exposed wooden surface: two beneath the gusset plate and one below the uncovered wooden surface, and an additional thermocouple was between the gusset plate and the wood surface. The obtained temperature data showed that soot-coated gusset plates absorb significantly more radiation and record higher temperatures within the specimens than the specimens with the bare gusset plates. It was also found that the bare gusset plate works as a protective layer for the wood at 20 kW/m2, but not at 10 and 15 kW/m2. The teeth certainly contributed to heat transfer increasing the temperatures within the wood higher than those without teeth, but the effect was only meaningful for the soot-covered specimens. Connection strength was also qualitatively analyzed and it was discovered that the bare specimen retained a strong connection between the gusset plate and wood. In contrast, the soot-coated specimen was easily removed by hand, even when exposed to the same heat flux. Applying these results to a realistic scenario, this loss in connection strength could result in truss failure and structural collapse, which may result in injury to or even death of the responding firefighters. Additional gusset plate protection measures may be necessary to prolong the connection strength and prevent structural collapse. Full article
(This article belongs to the Section Hazards and Sustainability)
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9 pages, 4813 KiB  
Proceeding Paper
Harvesting Human Energy to Power Head Torches Using a Thermoelectric Generator
by Elaf J. Majeed and Amani J. Majeed
Eng. Proc. 2024, 70(1), 30; https://doi.org/10.3390/engproc2024070030 - 7 Aug 2024
Viewed by 278
Abstract
People dissipate energy constantly, from their heartbeat to their footsteps. However, scientists are developing a technique for capturing power from human beings and converting it electricity that can power electronic medical devices or other devices that need low voltage. Energy harvesting and bioelectronics [...] Read more.
People dissipate energy constantly, from their heartbeat to their footsteps. However, scientists are developing a technique for capturing power from human beings and converting it electricity that can power electronic medical devices or other devices that need low voltage. Energy harvesting and bioelectronics researchers are currently exploring this form of energy recycling. Mechanical, chemical, and thermal energy are the three primary forms of energy in the human body. This paper focuses on thermal energy sources only, showing that the energy harvested from a person’s head can be used to power a headlamp. A total of seven thermoelectric generators (TEGs) were used, each comprising thirty-five thermocouples. An output voltage of 1.5 volts was obtained from the TEG systems. In addition, an electrical circuit was designed to convert the obtained TEG voltage into another voltage suitable for the headlamp model. Full article
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22 pages, 9040 KiB  
Article
Thermally Induced Moisture Flow in a Silty Sand under a 1-D Thermal Gradient
by Nice Kaneza, Aashish Pokhrel, Laureano R. Hoyos and Xinbao Yu
Geosciences 2024, 14(8), 207; https://doi.org/10.3390/geosciences14080207 - 2 Aug 2024
Viewed by 457
Abstract
Thermally induced moisture flow in unsaturated soils involves complex coupled thermal–hydro processes with the moisture flow in both the vapor and liquid phases. The accurate measurement of the moisture flow in unsaturated sands remains a challenging task due to low moisture migration, the [...] Read more.
Thermally induced moisture flow in unsaturated soils involves complex coupled thermal–hydro processes with the moisture flow in both the vapor and liquid phases. The accurate measurement of the moisture flow in unsaturated sands remains a challenging task due to low moisture migration, the temperature effect on moisture sensors, and the gravity effect on moisture flow. This study aims to accurately measure transient moisture flow, heat transfer, and thermal conductivity in a silty sand with 35% non-plastic fines in a closed heat cell with a controlled 1-D temperature gradient. The heat cell consists of two temperature-controlled heat exchanger plates, heat flux sensors, moisture sensors, thermocouples, and thermal conductivity sensors. The soil moisture sensors were calibrated in the test soil at room temperature and then at elevated incremental temperatures. Soil samples compacted at various initial moisture contents were tested under a constant 1-D temperature gradient of 4 °C/cm. Soil moisture redistribution, temperature, and thermal conductivity profiles were determined from the test results. Transient temperature responses indicated that a lower initial moisture content led to a higher temperature drop after reaching the peak, or a more concaved temperature profile in a steady state due to enhanced moisture migration driven by the temperature gradients. Dry soils exhibited uniform thermal properties, while moist soils showed varying thermal conductivity profiles. A critical moisture content was identified when the maximum moisture migration occurred. Thermal conductivity in soils increased with the distance from the heat source due to thermally induced moisture migration. These findings provide valuable insights into coupled moisture–heat flow dynamics in unsaturated sands. Full article
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11 pages, 3382 KiB  
Article
3D-Printed Conformal Thin Film Thermocouple Arrays for Distributed High-Temperature Measurements
by Jun Liu, Lida Xu, Xiong Zhou, Fuxin Zhao, Yusen Wang, Siqi Wang, Wenlong Lv, Daoheng Sun and Qinnan Chen
Coatings 2024, 14(8), 967; https://doi.org/10.3390/coatings14080967 - 2 Aug 2024
Viewed by 632
Abstract
Conformal thin film sensing represents a cutting-edge technology capable of precisely measuring complex surface temperature fields under extreme conditions. However, fabricating high-temperature-resistant conformal thin film thermocouple arrays remains challenging. This study reports a method for manufacturing conformal thin film thermocouple arrays on metal [...] Read more.
Conformal thin film sensing represents a cutting-edge technology capable of precisely measuring complex surface temperature fields under extreme conditions. However, fabricating high-temperature-resistant conformal thin film thermocouple arrays remains challenging. This study reports a method for manufacturing conformal thin film thermocouple arrays on metal spherical surfaces using a printable paste composed of silicates and Ag. Specifically, the use of silicate glass phases enhances the high-temperature performance of the silver printable paste, enabling the silver ink coatings to withstand temperatures up to 947 °C and survive over 25 h at 900 °C. The thermocouples, connected to Pt thin films, exhibited a Seebeck coefficient of approximately 17 μV/°C. As a proof of concept, an array of six Ag/Pt thin film thermocouples was successfully fabricated on a metal spherical surface. Compared to traditional wire-type thermocouples, the conformal thin film thermocouple arrays more accurately reflect temperature variations at different points on a spherical surface. The Ag/Pt conformal thin film thermocouple arrays hold promise for monitoring temperature fields in harsh environments, such as aerospace and nuclear energy applications. Full article
(This article belongs to the Special Issue Applications of Ceramic and Cermet Coatings)
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