Metal-chelating amino acids as building blocks for synthetic receptors sensing metal ions and histidine-tagged proteins

Chembiochem. 2003 Dec 5;4(12):1340-4. doi: 10.1002/cbic.200200455.

Abstract

Protein structure and function rely on a still not fully understood interplay of energetic and entropic constraints defined by the permutation of the twenty genetically encoded amino acids. Many attempts have been undertaken to design peptide-peptide interaction pairs and synthetic receptors de novo by using this limited number of building blocks. We describe a rational approach to creating a building block based on a tailored metal-chelating amino acid. Nepsilon,Nepsilon-bis(carboxymethyl)-L-lysine can be flexibly introduced into peptides by 9-fluorenylmethoxycarbonyl solid-phase chemistry. The corresponding metal-chelating peptides act as metal sensors and synthetic receptors for histidine-tagged proteins. These biochemical tweezers will open new ways to control protein-protein interactions, to design peptide-based interaction pairs, or to generate switchable protein function.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acids / chemistry*
  • Calcium / chemistry
  • Cations
  • Chelating Agents / chemistry*
  • Histidine / chemistry*
  • Magnesium / chemistry
  • Metals / analysis*
  • Nickel / chemistry
  • Peptides / analysis*
  • Peptides / chemistry
  • Receptors, Cell Surface / chemistry
  • Spectrometry, Fluorescence / methods

Substances

  • Amino Acids
  • Cations
  • Chelating Agents
  • Metals
  • Peptides
  • Receptors, Cell Surface
  • Histidine
  • Nickel
  • Magnesium
  • Calcium