Simple and rapid liquid chromatography method for determination of efavirenz in plasma

J Chromatogr B Analyt Technol Biomed Life Sci. 2006 May 1;835(1-2):131-5. doi: 10.1016/j.jchromb.2006.03.014. Epub 2006 Mar 29.

Abstract

A simple and rapid high performance liquid chromatographic method for determination of efavirenz in human plasma was developed. The method involved extraction of sample with ethyl acetate and analysis using a reversed-phase C(18) column (150 mm) with UV detection. The assay was linear from 0.0625 to 10.0 microg/ml. The method was specific for efavirenz estimation and the drug was stable in plasma up to one month at -20 degrees C. The average recovery of efavirenz from plasma was 101%. Due to its simplicity, the assay can be used for pharmacokinetic studies and therapeutic drug monitoring of efavirenz.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Alkynes
  • Anti-HIV Agents / blood
  • Benzoxazines
  • Chromatography, High Pressure Liquid / methods*
  • Cyclopropanes
  • Drug Stability
  • Humans
  • Oxazines / blood*
  • Reproducibility of Results
  • Sensitivity and Specificity

Substances

  • Alkynes
  • Anti-HIV Agents
  • Benzoxazines
  • Cyclopropanes
  • Oxazines
  • efavirenz