[HPLC determination of acteoside in Radix Rehmanniae]

Zhongguo Zhong Yao Za Zhi. 2006 May;31(10):822-4.
[Article in Chinese]

Abstract

Objective: To develop an HPLC method for the determination of acteoside in Radix Rehmanniae.

Method: The chromatographic conditions were as follows: Polaris C18(4.6 mm x 250 mm, 5 microm) column, a mobile phase in gradient mode composed of acetonitrile 0.1% acetic acid solution, a flow rate of 1.0 mL x min(-1), and 334 nm as the detection wavelength.

Result: Acteoside showed good linear relationship at the range of 10-500 microg x mL(-1) (r = 0.9990). The average recovery was 100.1%, RS D 3.7%.

Conclusion: The proposed method promised to be applicable for the quality control of Radix Rehmanniae.

MeSH terms

  • Chromatography, High Pressure Liquid / methods*
  • Glucosides / analysis*
  • Phenols / analysis*
  • Plant Roots / chemistry
  • Plants, Medicinal / chemistry*
  • Quality Control
  • Rehmannia / chemistry*
  • Reproducibility of Results
  • Sensitivity and Specificity

Substances

  • Glucosides
  • Phenols
  • acteoside