Solution structure of DNA containing alpha-OH-PdG: the mutagenic adduct produced by acrolein

Nucleic Acids Res. 2009 Apr;37(7):2153-63. doi: 10.1093/nar/gkp076. Epub 2009 Feb 17.

Abstract

Acrolein is a cell metabolic product and a main component of cigarette smoke. Its reaction with DNA produces two guanine lesions gamma-OH-PdG, a major adduct that is nonmutagenic in mammalian cells, and the positional isomer alpha-OH-PdG. We describe here the solution structure of a short DNA duplex containing a single alpha-OH-PdG lesion, as determined by solution NMR spectroscopy and restrained molecular dynamics simulations. The spectroscopic data show a mostly regular right-handed helix, locally perturbed at its center by the presence of the lesion. All undamaged residues of the duplex are in anti orientation, forming standard Watson-Crick base-pair alignments. Duplication of proton signals near the damaged site differentiates two enantiomeric duplexes, thus establishing the exocyclic nature of the lesion. At the lesion site, alpha-OH-PdG rotates to a syn conformation, pairing to its counter cytosine residue that is protonated at pH 5.9. Three-dimensional models produced by restrained molecular dynamics simulations show different hydrogen-bonding patterns between the lesion and its cytosine partner and identify further stabilization of alpha-OH-PdG in a syn conformation by intra-residue hydrogen bonds. We compare the alpha-OH-PdG.dC duplex structure with that of duplexes containing the analogous lesion propano-dG and discuss the implications of our findings for the mutagenic bypass of acrolein lesions.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Acrolein / toxicity*
  • DNA Adducts / chemistry*
  • Deoxycytidine / chemistry
  • Environmental Pollutants / toxicity*
  • Guanosine / analogs & derivatives*
  • Guanosine / chemistry
  • Models, Molecular
  • Mutagenesis
  • Nuclear Magnetic Resonance, Biomolecular
  • Protons
  • Lösungen

Substances

  • DNA Adducts
  • Environmental Pollutants
  • Protons
  • Lösungen
  • Deoxycytidine
  • Guanosine
  • Acrolein