Glaucocalyxin A inhibits platelet activation and thrombus formation preferentially via GPVI signaling pathway

PLoS One. 2013 Dec 30;8(12):e85120. doi: 10.1371/journal.pone.0085120. eCollection 2013.

Abstract

Platelets play a pivotal role in atherothrombosis and the antiplatelet agents have been proved to be useful in preventing onset of acute clinical events including myocardial infarction and stroke. Increasing number of natural compounds has been identified to be potential antiplatelet agents. Here we report the antiplatelet effect of glaucocalyxin A (GLA), an ent-diterpenoid that we isolated and purified from the aerial parts of Rabdosia japonica (Burm. f.) var. glaucocalyx (Maxim.) Hara, and investigate the molecular mechanisms by which GLA inhibits platelet activation and thrombus formation. The effect of GLA on platelet activation was measured using platelets freshly isolated from peripheral blood of healthy donors. Results showed that pretreatment of human platelets with lower concentrations of GLA (0.01 μg/ml, 0.1 μg/ml) significantly inhibited platelet aggregation induced by collagen (P<0.001) and CRP (P<0.01), a synthetic GPVI ligand, but not by ADP and U46619. Accordingly, GLA inhibited collagen-stimulated tyrosine phosphorylation of Syk, LAT, and phospholipase Cγ2, the signaling events in collagen receptor GPⅥ pathway. GLA also inhibited platelet p-selectin secretion and integrin activation by convulxin, a GPVI selective ligand. Additionally, GLA was found to inhibit low-dose thrombin-induced platelet activation. Using a flow chamber device, GLA was found to attenuate platelet adhesion on collagen surfaces in high shear condition. In vivo studies showed that GLA administration increased the time for complete occlusion upon vascular injury in mice, but did not extend tail-bleeding time when mice were administered with relatively lower doses of GLA. Therefore, the present results provide the molecular basis for the inhibition effect of GLA on platelet activation and its in vivo effect on thrombus formation, suggesting that GLA could potentially be developed as an antiplatelet and antithrombotic agent.

Publication types

  • Clinical Trial
  • Research Support, Non-U.S. Gov't

MeSH terms

  • 15-Hydroxy-11 alpha,9 alpha-(epoxymethano)prosta-5,13-dienoic Acid / pharmacology
  • Adenosine Diphosphate / pharmacology
  • Animals
  • Anti-Inflammatory Agents, Non-Steroidal / chemistry
  • Anti-Inflammatory Agents, Non-Steroidal / isolation & purification
  • Anti-Inflammatory Agents, Non-Steroidal / pharmacology*
  • Blood Coagulation / drug effects*
  • Blood Platelets / metabolism*
  • Collagen / pharmacology
  • Diterpenes, Kaurane / chemistry
  • Diterpenes, Kaurane / isolation & purification
  • Diterpenes, Kaurane / pharmacology*
  • Humans
  • Isodon / chemistry
  • Male
  • Mice
  • Platelet Adhesiveness / drug effects*
  • Platelet Membrane Glycoproteins / metabolism*
  • Signal Transduction
  • Vasoconstrictor Agents / pharmacology

Substances

  • Anti-Inflammatory Agents, Non-Steroidal
  • Diterpenes, Kaurane
  • Platelet Membrane Glycoproteins
  • Vasoconstrictor Agents
  • platelet membrane glycoprotein VI
  • Adenosine Diphosphate
  • 15-Hydroxy-11 alpha,9 alpha-(epoxymethano)prosta-5,13-dienoic Acid
  • glaucocalyxin A
  • Collagen

Grants and funding

This work was supported in part by grants from the National Science Foundation of China (NSFC81071410, NSFC81170132), Jiangsu Province’s Key Discipline of Medicine (XK201118), the Priority Academic Program Development of Jiangsu Higher Education Institutions of China (L.Z.). The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.