Immune responses to HBsAg conjugated to protein D of non-typeable Haemophilus influenzae in mice

PLoS One. 2015 Feb 17;10(2):e0117736. doi: 10.1371/journal.pone.0117736. eCollection 2015.

Abstract

Background: Hepatitis B vaccine that contains an aluminum hydroxide adjuvant induces apoptotic death of Hepa 1-6 cells. Difficult-to-degrade chemical additives in vaccines effectively enhance vaccine immunogenicity, but also affect the host tissue. Identification of bio-molecules that are readily degraded and compatible in vivo as an adjuvant is important for vaccine research. The hapten-carrier effect suggests that stimulation of helper T (Th) cells by carrier adjuvants is feasible. Protein D (PD) of non-typeable Haemophilus influenzae covalently conjugated to some polysaccharide vaccines has been confirmed to convert T-cell independent (TI) antigens into T-cell dependent (TD) antigens, and elicit strong T-cell responses ultimately. Herein, we would substitube PD for aluminum hydroxide adjuvant in Hepatitis B vaccine.

Methods and results: Truncated PD (amino acids 20-364) was expressed in Escherichia coli and purified by (NH4)2SO4 precipitation and DEAE chromatography. After evaluation of antigenicity by western blotting, PD was covalently conjugated to yeast-derived recombinant HBsAg by cross-linking with glutaraldehyde. Intramuscular immunization with the conjugate induced higher level of HBsAg-specific antibody than did HBsAg alone (p < 0.05), and was comparable to commercial Hepatitis B vaccine. During the surveillance period (days 35-105), anti-HBs titers were hold high. Moreover, the conjugated vaccine enhanced Th1 immune responses, while Th2 responses were also activated and induced an antibody response, as determined by IFN-γ ELISPOT and IgG1/IgG2a ratio assays.

Conclusions: Recombinant truncated PD covalently conjugated to HBsAg antigen enhanced the immunogenicity of the antigen in mice simultaneously by humoral and cellular immune response, which would facilitate therapeutic hepatitis B vaccines.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antibodies, Viral / immunology
  • B-Lymphocytes / cytology
  • B-Lymphocytes / immunology
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism*
  • CD4-Positive T-Lymphocytes / immunology
  • CD8-Positive T-Lymphocytes / immunology
  • Carrier Proteins / genetics
  • Carrier Proteins / metabolism*
  • Cell Communication / immunology
  • Female
  • Haemophilus influenzae / classification
  • Haemophilus influenzae / immunology*
  • Hepatitis B Surface Antigens / immunology*
  • Hepatitis B Surface Antigens / metabolism
  • Immunoconjugates / immunology*
  • Immunoglobulin D / genetics
  • Immunoglobulin D / metabolism*
  • Immunoglobulin G / immunology
  • Lipoproteins / genetics
  • Lipoproteins / metabolism*
  • Mice
  • Plasmids / genetics
  • Spleen / immunology
  • T-Lymphocytes, Helper-Inducer / cytology
  • T-Lymphocytes, Helper-Inducer / immunology
  • Viral Vaccines / immunology

Substances

  • Antibodies, Viral
  • Bacterial Proteins
  • Carrier Proteins
  • Hepatitis B Surface Antigens
  • Immunoconjugates
  • Immunoglobulin D
  • Immunoglobulin G
  • Lipoproteins
  • Viral Vaccines
  • glpQ protein, Haemophilus influenzae

Grants and funding

This work was supported by a grant from the Chinese Ministry of Science and Technology Program for Important Infectious Diseases Control and Prevention (2012ZX10002-001). The funders had no role in study design, data collection and analysis, decision to publish, or preparation of the manuscript.