Cell uptake, intracellular distribution, fate and reactive oxygen species generation of polymer brush engineered CeO(2-x) NPs

Nanoscale. 2015 Apr 21;7(15):6588-98. doi: 10.1039/c5nr00884k.

Abstract

Cerium Oxide nanoparticles (CeO(2-x) NPs) are modified with polymer brushes of negatively charged poly (3-sulfopropylmethacrylate) (PSPM) and positively charged poly (2-(methacryloyloxy)ethyl-trimethylammonium chloride) (PMETAC) by Atom Transfer Radical Polymerisation (ATRP). CeO(2-x) NPs are fluorescently labelled by covalently attaching Alexa Fluor® 488/Fluorescein isothiocyanate to the NP surface prior to polymerisation. Cell uptake, intracellular distribution and the impact on the generation of intracellular Reactive Oxygen Species (ROS) with respect to CeO(2-x) NPs are studied by means of Raman Confocal Microscopy (CRM), Transmission Electron Microscopy (TEM) and Inductively Coupled Plasma Mass Spectroscopy (ICP-MS). PSPM and PMETAC coated CeO(2-x) NPs show slower and less uptake compared to uncoated Brush modified NPs display a higher degree of co-localisation with cell endosomes and lysosomes after 24 h of incubation. They also show higher co-localisation with lipid bodies when compared to unmodified CeO(2-x) NPs. The brush coating does not prevent CeO(2-x) NPs from displaying antioxidant properties.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Apoptosis
  • Cell Lineage
  • Cell Separation
  • Cerium / chemistry*
  • Colloids / chemistry
  • Flow Cytometry
  • Fluorescein-5-isothiocyanate / chemistry
  • HEK293 Cells
  • Humans
  • Mass Spectrometry
  • Metal Nanoparticles / chemistry*
  • Methacrylates / chemistry
  • Microscopy, Confocal
  • Microscopy, Electron, Transmission
  • Polymers / chemistry*
  • Reactive Oxygen Species / chemistry*
  • Spectrum Analysis, Raman

Substances

  • 2-(trimethylammonio)ethyl methacrylate
  • Colloids
  • Methacrylates
  • Polymers
  • Reactive Oxygen Species
  • poly(3-sulfopropylmethacrylate)
  • Cerium
  • ceric oxide
  • Fluorescein-5-isothiocyanate