A Study of Liposomal Formulations to Improve the Delivery of Aquated Cisplatin to a Multidrug Resistant Tumor

Pharm Res. 2015 Oct;32(10):3261-8. doi: 10.1007/s11095-015-1702-6. Epub 2015 May 12.

Abstract

Purpose: This study was aimed at exploring the use of liposomes to deliver aquated cisplatin (ACP), a metabolite of CDDP, with increased potency and toxicity. Three liposomal formulations were compared for delivery of ACP to a multidrug resistant tumor.

Methods: Three different liposomes (DMPC, DPPC and DSPC as the main lipid components) were loaded with ACP by the thin-film hydration method. In vitro drug release was assessed over 72 h at 37°C in PBS. The pharmacokinetics of free CDDP and the three ACP liposomes was determined using ICP-AES and their efficacy against EMT6-AR1 multidrug resistant murine breast tumor was compared.

Results: The DSPC formulation, composed of a C18 acyl chain lipid, exhibited the slowest drug release (~2%) after 72 h at 37°C, compared to the other two formulations with decreased carbon chain lengths (C16 and C14; 7 and 25% release respectively). The pharmacokinetic profile was improved with all liposomal formulations relative to free CDDP, with clearance reduced by 500-fold for DSPC, 200-fold for DPPC and 130-fold for DMPC. The DSPC formulation displayed the highest drug accumulation in the tumor with 2-fold, 3-fold and 100-fold increases compared to DPPC, DMPC and free CDDP respectively. The DSPC formulation significantly inhibited the EMT6-AR1 tumor growth by ~90%, while the other formulations displayed no statistically significant improved activity compared to saline.

Conclusion: These results suggest that the DSPC liposomal formulation is a promising formulation for MDR tumor therapy over DMPC and DPPC formulations and free drug.

Keywords: aquated cisplatin; cisplatin; long circulating liposome; multidrug resistant tumor.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Cell Proliferation / drug effects
  • Chemistry, Pharmaceutical / methods
  • Cisplatin / chemistry*
  • Cisplatin / pharmacology*
  • Drug Carriers / chemistry
  • Drug Resistance, Neoplasm / drug effects*
  • Female
  • Liposomes / chemistry*
  • Mice
  • Mice, Inbred BALB C
  • Neoplasms / drug therapy*
  • Phosphatidylcholines / chemistry
  • Tissue Distribution / drug effects

Substances

  • Drug Carriers
  • Liposomes
  • Phosphatidylcholines
  • Cisplatin