Synthesis and biological evaluation of several dephosphonated analogues of CMP-Neu5Ac as inhibitors of GM3-synthase

Chemistry. 2015 Oct 5;21(41):14614-29. doi: 10.1002/chem.201501770. Epub 2015 Aug 11.

Abstract

Previous studies demonstrated that reducing the GM3 content in myoblasts increased the cell resistance to hypoxic stress, suggesting that a pharmacological inhibition of the GM3 synthesis could be instrumental for the development of new treatments for ischemic diseases. Herein, the synthesis of several dephosphonated CMP-Neu5Ac congeners and their anti-GM3-synthase activity is reported. Biological activity testes revealed that some inhibitors almost completely blocked the GM3-synthase activity in vitro and reduced the GM3 content in living embryonic kidney 293A cells, eventually activating the epidermal growth factor receptor (EGFR) signaling cascade.

Keywords: glycosides; inhibitors; sialic acids; sphingolipids.

MeSH terms

  • Cytidine Monophosphate / analogs & derivatives*
  • Cytidine Monophosphate / chemical synthesis
  • Cytidine Monophosphate / chemistry
  • Cytidine Monophosphate N-Acetylneuraminic Acid / chemistry*
  • Cytidine Monophosphate N-Acetylneuraminic Acid / metabolism
  • Enzyme Inhibitors / chemical synthesis*
  • Enzyme Inhibitors / chemistry*
  • ErbB Receptors / chemistry*
  • Humans
  • Kidney / chemistry
  • Kidney / enzymology*
  • Sialic Acids / chemical synthesis*
  • Sialic Acids / chemistry*
  • Sialyltransferases / antagonists & inhibitors*
  • Sialyltransferases / chemistry*
  • Sialyltransferases / metabolism
  • Signal Transduction / drug effects

Substances

  • Enzyme Inhibitors
  • Sialic Acids
  • cytidine-5'-monophosphosialic acid
  • Cytidine Monophosphate N-Acetylneuraminic Acid
  • Sialyltransferases
  • haematoside synthetase
  • ErbB Receptors
  • Cytidine Monophosphate