Computational and experimental analysis of short peptide motifs for enzyme inhibition

PLoS One. 2017 Aug 15;12(8):e0182847. doi: 10.1371/journal.pone.0182847. eCollection 2017.

Abstract

The metabolism of living systems involves many enzymes that play key roles as catalysts and are essential to biological function. Searching ligands with the ability to modulate enzyme activities is central to diagnosis and therapeutics. Peptides represent a promising class of potential enzyme modulators due to the large chemical diversity, and well-established methods for library synthesis. Peptides and their derivatives are found to play critical roles in modulating enzymes and mediating cellular uptakes, which are increasingly valuable in therapeutics. We present a methodology that uses molecular dynamics (MD) and point-variant screening to identify short peptide motifs that are critical for inhibiting β-galactosidase (β-Gal). MD was used to simulate the conformations of peptides and to suggest short motifs that were most populated in simulated conformations. The function of the simulated motifs was further validated by the experimental point-variant screening as critical segments for inhibiting the enzyme. Based on the validated motifs, we eventually identified a 7-mer short peptide for inhibiting an enzyme with low μM IC50. The advantage of our methodology is the relatively simplified simulation that is informative enough to identify the critical sequence of a peptide inhibitor, with a precision comparable to truncation and alanine scanning experiments. Our combined experimental and computational approach does not rely on a detailed understanding of mechanistic and structural details. The MD simulation suggests the populated motifs that are consistent with the results of the experimental alanine and truncation scanning. This approach appears to be applicable to both natural and artificial peptides. With more discovered short motifs in the future, they could be exploited for modulating biocatalysis, and developing new medicine.

MeSH terms

  • Amino Acid Motifs
  • Binding Sites
  • Enzyme Activation / drug effects
  • Enzyme Inhibitors / chemistry
  • Enzyme Inhibitors / pharmacology
  • Inhibitory Concentration 50
  • Molecular Dynamics Simulation
  • Peptides / chemistry*
  • Peptides / pharmacology
  • Protein Binding
  • Protein Structure, Secondary
  • beta-Galactosidase / antagonists & inhibitors

Substances

  • Enzyme Inhibitors
  • Peptides
  • beta-Galactosidase

Grants and funding

This work was supported by an Army Research Office YIP award to J.F. (W911NF-14-1-0434), the Cottrell College Science Award to J.F. Drs. Fu and Larini are also supported by the start-up funds from Rutgers University-Camden. This work used the Extreme Science and Engineering Discovery Environment (XSEDE)(grant no. MCB150005 to L.L), which is supported by National Science Foundation. This study used the computational resources provided by the Center for Computational and Integrative Biology (CCIB) through the National Science Foundation (grant no. DBI-1126052).