Multiple Hotspot Mutations Scanning by Single Droplet Digital PCR

Clin Chem. 2018 Feb;64(2):317-328. doi: 10.1373/clinchem.2017.272518. Epub 2017 Nov 9.

Abstract

Background: Progress in the liquid biopsy field, combined with the development of droplet digital PCR (ddPCR), has enabled noninvasive monitoring of mutations with high detection accuracy. However, current assays detect a restricted number of mutations per reaction. ddPCR is a recognized method for detecting alterations previously characterized in tumor tissues, but its use as a discovery tool when the mutation is unknown a priori remains limited.

Methods: We established 2 ddPCR assays detecting all genomic alterations within KRAS exon 2 and EGFR exon 19 mutation hotspots, which are of clinical importance in colorectal and lung cancer, with use of a unique pair of TaqMan® oligoprobes. The KRAS assay scanned for the 7 most common mutations in codons 12/13 but also all other mutations found in that region. The EGFR assay screened for all in-frame deletions of exon 19, which are frequent EGFR-activating events.

Results: The KRAS and EGFR assays were highly specific and both reached a limit of detection of <0.1% in mutant allele frequency. We further validated their performance on multiple plasma and formalin-fixed and paraffin-embedded tumor samples harboring a panel of different KRAS or EGFR mutations.

Conclusions: This method presents the advantage of detecting a higher number of mutations with single-reaction ddPCRs while consuming a minimum of patient sample. This is particularly useful in the context of liquid biopsy because the amount of circulating tumor DNA is often low. This method should be useful as a discovery tool when the tumor tissue is unavailable or to monitor disease during therapy.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biopsy
  • Circulating Tumor DNA / blood
  • ErbB Receptors / genetics*
  • Genes, ras*
  • Humans
  • Limit of Detection
  • Liquid Biopsy
  • Molecular Probes
  • Mutation*
  • Neoplasms / blood
  • Neoplasms / genetics*
  • Neoplasms / pathology
  • Polymerase Chain Reaction / methods*

Substances

  • Circulating Tumor DNA
  • Molecular Probes
  • ErbB Receptors