Application of the DP4 Probability Method to Flexible Cyclic Peptides with Multiple Independent Stereocenters: The True Structure of Cyclocinamide A

Org Lett. 2018 Jul 20;20(14):4314-4317. doi: 10.1021/acs.orglett.8b01756. Epub 2018 Jul 9.

Abstract

A DP4 protocol has been successfully utilized to establish the true structure of the natural product cyclocinamide A, a flexible cyclic peptide with four isolated stereocenters. Benchmarking the necessary level of theory required to successfully predict the NMR spectra of three previously synthesized isomers of cyclocinamide A led to the prediction of the natural stereochemistry as 4 S, 7 R, 11 R, 14 S, which has been confirmed by total synthesis.

Publication types

  • Research Support, N.I.H., Extramural

MeSH terms

  • Computers, Molecular
  • Glycine / chemistry
  • Molecular Structure
  • Peptides, Cyclic / chemistry*
  • Probability
  • Pyrroles / chemistry
  • Stereoisomerism

Substances

  • Peptides, Cyclic
  • Pyrroles
  • cyclocinamide A
  • Glycine