A step towards development of promising trypanocidal agents: Synthesis, characterization and in vitro biological evaluation of ferrocenyl Mannich base-type derivatives

Eur J Med Chem. 2019 Feb 1:163:569-582. doi: 10.1016/j.ejmech.2018.12.005. Epub 2018 Dec 4.

Abstract

Chagas disease is a neglected chronical parasitosis caused by the parasite Trypanosoma cruzi (T. cruzi). Nine ferrocenyl Mannich base derivatives were synthetized and characterized to explore their in vitro activity on three T. cruzi strains of the parasite and their cytotoxicity on Vero cells to calculate the selectivity index (SI). Compound 2, 1-ferrocenyl-3-(4-(4-(trifluoromethyl)phenyl)piperazin-1-yl)propan-1-one, stood out as the most promising derivative showing a half maximal inhibitory concentration (IC50) value around 5 μM in both amastigote and trypomastigote forms of T. cruzi and SI values higher than 13, being the best value on the trypomastigote forms of the Arequipa strain (SI = 41.7). Moreover, 2 decreased the number of infected cells and was not genotoxic. Furthermore, its possible mechanism of action was studied through the alteration of the metabolites excreted by the parasite during glucose metabolism, the detection of mitochondrial alterations and the inhibition of superoxide dismutase (SOD). Finally, docking studies were executed to analyze the binding mode of the studied compounds to Fe-SOD enzyme.

Keywords: Chagas disease; Ferrocene; In vitro studies; Mannich bases; Superoxide dismutase; Trypanosoma cruzi.

MeSH terms

  • Animals
  • Chagas Disease / drug therapy*
  • Chlorocebus aethiops
  • Glucose Metabolism Disorders
  • Mannich Bases / chemical synthesis
  • Mannich Bases / pharmacology*
  • Molecular Docking Simulation
  • Protein Binding
  • Superoxide Dismutase / metabolism
  • Trypanocidal Agents / chemical synthesis*
  • Trypanocidal Agents / pharmacology
  • Trypanosoma cruzi / enzymology
  • Trypanosoma cruzi / metabolism
  • Vero Cells / parasitology

Substances

  • Mannich Bases
  • Trypanocidal Agents
  • Superoxide Dismutase