Lewis Acid-Catalyzed Intermolecular Annulation: Three-Component Reaction toward Imidazo[1,2- a]pyridine Thiones

J Org Chem. 2019 Jul 19;84(14):9369-9377. doi: 10.1021/acs.joc.9b01188. Epub 2019 Jul 5.

Abstract

A Lewis acid-catalyzed three-component annulation reaction of 2-aminopyridines and ynals with elemental sulfur was established. A series of imidazo[1,2-a]pyridine thiones was obtained in moderate to excellent yields. The merits of this transformation include easily available starting materials, multiple C-heteroatom bond formation in one pot, good functional group tolerance, elemental sulfur as S source, operational simplicity, etc.