Conducting polymer functionalized Cu-metal organic framework-based electrochemical immunosensor for rapid and sensitive quantitation of Escherichia coli O157:H7

Mikrochim Acta. 2024 Nov 13;191(12):740. doi: 10.1007/s00604-024-06807-1.

Abstract

Escherichia coli (E. coli) O157:H7 is an important food-borne pathogen that can cause hemorrhagic diarrhea and enteritis in humans and animals. Realizing the rapid quantitation of E. coli O157:H7 is of great significance for the guarantee of food safety and disease control. In this study, an electrochemical immunosensing technique based on a functionalized composite of Cu-metal organic framework (Cu-MOF) and poly (3,4-ethylenedioxythiophene)-poly (styrenesulfonate) (PEDOT:PSS) is developed, achieving rapid and sensitive quantitation of E. coli O157:H7 in food and clinical feces samples. The organic functionalization of Cu-MOF significantly improves the interface conductivity to facilitate electron transfer and provides the sulfonic groups (-SO3H) to conjugate bio-recognizing elements for target determination. The immunosensor delivers a linear detection range of 3 × 102 ~ 3 × 108 cfu/mL, a low limit of detection (LOD) of 7.4 cfu/mL, and a short analysis time of 40 min. In addition, it does not show any cross-reactivity with other common pathogens and exhibits high repeatability with relative standard deviations (RSDs) all lower than 2.09%, providing a promising approach for warranting food safety and control of E. coli O157:H7 disease.

Keywords: E. coli O157:H7; Cu-metal organic framework; Electrochemical immunosensor; Electrochemical impedance spectroscopy; Modified glassy carbon electrode; Organic functionalization.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antibodies, Immobilized / chemistry
  • Antibodies, Immobilized / immunology
  • Biosensing Techniques / methods
  • Bridged Bicyclo Compounds, Heterocyclic / chemistry
  • Copper* / chemistry
  • Electrochemical Techniques* / methods
  • Escherichia coli O157* / immunology
  • Escherichia coli O157* / isolation & purification
  • Feces / chemistry
  • Feces / microbiology
  • Humans
  • Immunoassay / methods
  • Limit of Detection*
  • Metal-Organic Frameworks* / chemistry
  • Polymers / chemistry
  • Polystyrenes / chemistry

Substances

  • Metal-Organic Frameworks
  • Copper
  • poly(3,4-ethylene dioxythiophene)
  • Antibodies, Immobilized
  • Bridged Bicyclo Compounds, Heterocyclic
  • Polystyrenes
  • Polymers