Validity testing of the accuPINCH THC test

J Anal Toxicol. 1995 Jan-Feb;19(1):5-12. doi: 10.1093/jat/19.1.5.

Abstract

Self-contained drug-testing kits are currently being marketed for a variety of drugs of abuse. These tests are designed to provide rapid access to test results without the need for laboratory facilities. This report describes a validity study of the accuPINCH THC test, a self-contained test for cannabinoids in urine. Three healthy male volunteers with a history of marijuana use participated in the clinical study. Each subject smoked one, two, or four marijuana cigarettes (2.6% THC) on each test day. Urine samples were collected and incorporated into a specimen set consisting of 178 clinical samples, 72 urine samples containing known amounts of drug, and 50 drug-free urine samples. The specimen set was randomized and analyzed under blind conditions by the accuPINCH test and by gas chromatography-mass spectrometry (GC-MS) for 11-nor-9-carboxy-delta 9-tetrahydrocannabinol (THCCOOH). AccuPINCH results were interpreted independently by three readers as positive at either two calibration points (positive A < 100 ng/mL THCCOOH; positive B > or = 100 ng/mL THCCOOH) or negative. Concordance analysis was performed by comparison of the accuPINCH results with GC-MS. In addition, the effects of changes in sample turbidity, temperature, and assay reading time on test outcome were assessed. For the clinical samples, positive B results were associated exclusively with THCCOOH concentrations greater than or equal to 15 ng/mL, whereas positive A and negative results were obtained at all concentrations. All drug-free urine samples were interpreted as either negative or positive A. The test demonstrated relatively low cross-reactivity with THC and other cannabinoids.(ABSTRACT TRUNCATED AT 250 WORDS)

Publication types

  • Clinical Trial
  • Comparative Study

MeSH terms

  • Adult
  • Cannabinoids / urine*
  • Dronabinol / analogs & derivatives*
  • Dronabinol / urine
  • Gas Chromatography-Mass Spectrometry
  • Humans
  • Immunoenzyme Techniques
  • Male
  • Marijuana Abuse / diagnosis*
  • Marijuana Smoking / urine*
  • Middle Aged
  • Random Allocation
  • Reagent Kits, Diagnostic / standards
  • Reference Standards
  • Reproducibility of Results
  • Sensitivity and Specificity
  • Temperature

Substances

  • Cannabinoids
  • Reagent Kits, Diagnostic
  • 11-nor-delta(9)-tetrahydrocannabinol-9-carboxylic acid
  • Dronabinol