Investigating highly crosslinked macroporous resins for solid-phase synthesis

Bioorg Med Chem Lett. 1998 Sep 8;8(17):2363-8. doi: 10.1016/s0960-894x(98)00427-2.

Abstract

The washing efficiencies of a chromophore and the reaction rates of a classical esterification reaction are improved with macroporous resins (MRs) relative to a classical Merrifield resin. Furthermore, Wacker-oxidation of a MR bound alkene yielded the expected methylketone product whereas an alkene bound to a low-crosslinked Merrifield resin gave no product, a function of the relative permeability of each of these resins to the aqueous solvent conditions employed.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Cross-Linking Reagents
  • Drug Design
  • Esters / chemical synthesis*
  • Esters / chemistry
  • Ketones / chemical synthesis*
  • Ketones / chemistry
  • Kinetics
  • Molecular Conformation
  • Molecular Structure
  • Resins, Synthetic*
  • Structure-Activity Relationship
  • Surface Properties

Substances

  • Cross-Linking Reagents
  • Esters
  • Ketones
  • Resins, Synthetic